Experimental Organic Chemistry: Standard and Microscale

This established text continues to provide a rigorous account of the principles and practice of experimental organic chemistry, taking students from their first day in the laboratory right through to research work. New to this edition, a microscale approach has been integrated into the entire text, alongside conventional manipulations, bringing it in line with current laboratory practice. Maintaining the unique structure of the previous edition, the first half of the book surveys all aspects of safe laboratory practice, the use of a wide range of purification and analytical techniques, particularly spectroscopic analysis. The second half contains easy–to–follow experimental procedures, each designed to illustrate an important reaction type of basic principle of organic chemistry. Tried and tested over the past decade, these experiments are graded according to their complexity and many of these have microscale equivalents. Of prime importance, all aspects of health and safety in the laboratory have been updated according to the latest guidelines and are highlighted throughout the text.

Spis treści:
Preface.
Part 1: Laboratory Practice.
1 Safety in the Chemical Laboratory.
2 Glasware and Equipment in the Laboratory.
3 Organic Reactions: from Starting Materials to Pure Organic Product.
4 Qualitative Analysis of Organic Compounds.
5 Spectroscopic Analysis of Organic Compounds.
6 Keeping Records: the Laboratory Notebook and Chemical Literature.
Part 2: Experimental Procedures.
Introduction.
List of Experiments.
Experiments which can be Taken in Sequence.
Experiments which Illustrate Particular Techniques.
7 Functional Group Interconversions.
8 Carbon – Carbon Bond–Forming Reactions.
9 Projects.
Appendices.
Index of Chemicals.
General Index

Nota biograficzna:
Laurence Harwood is Professor of Organic Chemistry in the School of Chemistry, Unive rsity of Reading, Christopher Moody is Sir Jesse Boot Professor of Chemistry in the School of Chemistry, University of Nottingham and Jonathan Percy is Professor of Chemistry in the Department of Chemistry, University of Leicester

Okładka tylna:
This established text continues to provide a rigorous account of the principles and practice of experimental organic chemistry, taking students from their first day in the laboratory right through to research work. New to this edition, a microscale approach has been integrated into the entire text, alongside conventional manipulations, bringing it in line with current laboratory practice. Maintaining the unique structure of the previous edition, the first half of the book surveys all aspects of safe laboratory practice, the use of a wide range of purification and analytical techniques, particularly spectroscopic analysis. The second half contains easy–to–follow experimental procedures, each designed to illustrate an important reaction type of basic principle of organic chemistry. Tried and tested over the past decade, these experiments are graded according to their complexity and many of these have microscale equivalents. Of prime importance, all aspects of health and safety in the laboratory have been updated according to the latest guidelines and are highlighted throughout the text.