Experimental Organic Chemistry

This cutting–edge lab manual takes a multiscale approach, presenting both micro, semi–micro, and macroscale techniques. The manual is easy to navigate with all relevant techniques found as they are needed. Cutting–edge subjects such as HPLC, bioorganic chemistry, multistep synthesis, and more are presented in a clear and engaging fashion.

Spis treści:
THE BASICS.
Laboratory Safety.
Basic Concepts.
Basic Operations.
THE EXPERIMENTS.
Recrystallization and Melting Point.
Extraction.
Distillation–Seperation and Purification of Organic Liquids.
Gas Chromatography.
Thin–Layer Chromatography.
Column Chromatography.
High–Performance Liquid Chromatography.
Refractometry and Polarimetry.
Alcohols and Alkenes.
Alkyl Halides.
Acid–Base Extraction.
Phenols and Ethers.
Electrophilic Aromatic Substitution.
Nucleophilic Aromatic Substitution.
Chemical Kinetics.
Diels–Alder Reaction.
Aldehydes and Ketones.
Oxidation–Reduction.
Esters.
Multistep Synthesis.
Molecules of Life.
Lipids.
Polymers.
Dyes and Pigments.
Bioorganic Chemistry.
Molecules of Heredity.
SPECTROSCOPY.
Absorption Spectroscopy.
Infrared Spectroscopy.
Ultraviolet–Visible Spectroscopy.
Nuclear Magnetic Resonance.
Mass Spectroscopy.
Answers to Odd–Numbered Exercises.
Credits.
Index.