Organic Syntheses, Collective Volume 9

Reflecting the increased pace of research and the many recent advances in organic chemistry, this series serves as a single–source compendium of the most up–to–date and significant procedures currently in use. Volume 9 consists of checked procedures previously published in annual volumes, revised and updated.

Spis treści:
Partial table of contents:
Synthesis of 2–Substituted Naphthalenediol Derivatives Using Chromium Carbene Complexes: 1–Acetoxy–2–Butyl–4–Methoxynaphthalene.
Highly Reactive Calcium for the Preparation of Organocalcium Reagents: Preparation of 1–Adamantylcalcium Halides and Their Addition to Ketones: 1–(1–Adamantyl) Cycohexanol.
Bis(Trifluoroethyl)(Carboethoxymethyl)Phosphonate.
N–tert––Butoxycarbonyl–2–Bromopyrrole.
Allylic Alcohols by Alkene Transfer from Zirconium to Zinc: 1–[(tert–Butyldiphenylsilyl)Oxy]–Dec–3–En–5–Ol.
1,3,5–Cyclooctatriene.
Diethyl 1–Propyl–2–Oxoethylphosphonate.
3, 4–Diethylpyrrole.
Dialkyl Mesoxalates by Ozonolysis of Dialkyl Benzalmalonates: Dimethyl Mesoxalate.
Manganese–Copper–Catalyzed Conjugate Addition of Organomagnesium Reagents to ,beta–Ethylenic Ketones: 2–(1,1–Dimethylpentyl)–5–Methyl Cyclohexanone.
4–Dodecylbenzenesulfonyl Azides.
Ethyl 2–Methyl–5–Phenyl–3–Furancarboxylate.
Preparation and Reactions of Alkenylchromium Reagents: 2–Hexyl–5–Phenyl–1–Penten–3–OL.
Preparation and Use of (Methoxymethoxy)Methyllithium: 1–(Hydroxymethyl) Cycloheptanol.
Acetylenic Ethers from Alcohols and Their Reduction to Z– and E–Enol Ethers: 1–Menthoxy–1–Butyne.
Methyl 5–Methoxyindole–2–Acetate.
A General Method for the Pre paration of –Branched Amino Acids: (S)–2–Methyl Proline.
Synthesis of Epoxides Using Dimethyldioxirane: trans–Stilbene Oxide.
Tris(Trimethylsilyl)Silane.
Indexes.